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Sample Record for 2022-09-20-1

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Project Information

Project ID: 55555 DEA: AMRL EFIS: AMRL QA Service Level:
DIST-CO-RTE-PM: 59---
Work Description: Special project for submitting Sample information for AASHTO Materials Reference Laboratory (AMRL).
Location Description:
Contractor Name: Unknown
Contractor Address: Unknown
Resident Engineer: Unknown Structure Rep.: Unknown

Sample Information

DIME Sample ID: 2022-09-20-1
TL Number from the TL Form:
Sample Submitted By Organization: CT HQ - Sacramento Asphalt Binder Laboratory
Sample Organization Contact: (916) 227-7302
Type of Sample: Proficiency
Type of Material: Asphalt Binder
Sample Taken Date: 09/20/2022
Date that the sample was received by the laboratory/organization performing the testing: 09/19/2022
The quantity of what the sample constitutes: 1 can
A brief description of the sample: 269 (A)
From where was the sample collected: Manufacturer
Laboratory sample identification:
Structure unique identifier:
Structure name:
The fabricator/manufacturer/facility name: AASHTO Resouces

Material Information

Performance Grade: PG 76-22 M
Modified: Yes
Lot number:
Sublot number:
Tank number:
Time of sample:
HMA Supplier:
Certified Asphalt Supplier: AASHTO Resource - Frederick MD
Multigrade: No
Multigrade Type:
Asphalt Binder Mix Number:
Test results on following page(s): 17

Test Results

Test 1 of 17

DIME Test ID: 2022-09-20-1-1
Test Method: AASHTO T240-17: Standard Method of Test for Effect of Heat and Air on a Moving Film of Asphalt Binder (Rolling Thin-Film Oven Test)
Verified Date: 09/20/2022
Date Tested: 09/20/2022
Submitted By Organization: CT HQ - Sacramento Asphalt Binder Laboratory
Organization Address: 5900 Folsom Boulevard, Room 225,
Organization City: Sacramento
Organization State: CA
Organization Zipcode: 95819
Organization Email: guadalupe.magana@dot.ca.gov
Organization Phone: (916) 227-7302
General Comments for this Test: Mass Change
Test Result Compliance: complies
Additional Comments When Verified:
Is mass change based on one or two containers? Two
Any material loss from containers during heating process/testing? No
Mass of empty container #1 171.144 grams
Mass of empty container #2 158.955 grams
Mass of container #1 before test (m1i) 206.224 grams
Mass of container #2 before test (m2i) 194.040 grams
Mass of container #1 after test (m1f) 206.138 grams
Mass of container #2 after test (m2f) 193.957 grams
Average mass change -0.241 percent

Test 2 of 17

DIME Test ID: 2022-09-20-1-2
Test Method: AASHTO T301-22: Standard Method of Test for Elastic Recovery Test of Asphalt Materials by Means of a Ductilometer
Verified Date: 09/22/2022
Date Tested: 09/21/2022
Submitted By Organization: CT HQ - Sacramento Asphalt Binder Laboratory
Organization Address: 5900 Folsom Boulevard, Room 225,
Organization City: Sacramento
Organization State: CA
Organization Zipcode: 95819
Organization Email: guadalupe.magana@dot.ca.gov
Organization Phone: (916) 227-7302
General Comments for this Test: ER
Test Result Compliance: complies
Additional Comments When Verified:
% Elongation Recovery 96 %

Test 3 of 17

DIME Test ID: 2022-09-20-1-3
Test Method: AASHTO T315-22: Standard Method of Test for Determining the Rheological Properties of Asphalt Binder Using a Dynamic Shear Rheometer (DSR) (Dynamic Shear)
Verified Date: 09/20/2022
Date Tested: 09/20/2022
Submitted By Organization: CT HQ - Sacramento Asphalt Binder Laboratory
Organization Address: 5900 Folsom Boulevard, Room 225,
Organization City: Sacramento
Organization State: CA
Organization Zipcode: 95819
Organization Email: guadalupe.magana@dot.ca.gov
Organization Phone: (916) 227-7302
General Comments for this Test: OG
Test Result Compliance: complies
Additional Comments When Verified:
Phase Original binder
Test Gap 1 mm
Test Frequency 10.0 rad/s
Strain Amplitude 12.00 %
Stress Amplitude 0.155 kPa
Phase Angle (δ) (for the 10 cycles) 46.2 degree
Complex Modulus (G*) (for the 10 measurements) 1.294 kPa
Test Temperature (Specimen 1) 76.0 C
Dynamic Shear, G*/sin(δ) 1.79 kPa

Test 4 of 17

DIME Test ID: 2022-09-20-1-4
Test Method: AASHTO T315-22: Standard Method of Test for Determining the Rheological Properties of Asphalt Binder Using a Dynamic Shear Rheometer (DSR) (Dynamic Shear)
Verified Date: 09/20/2022
Date Tested: 09/20/2022
Submitted By Organization: CT HQ - Sacramento Asphalt Binder Laboratory
Organization Address: 5900 Folsom Boulevard, Room 225,
Organization City: Sacramento
Organization State: CA
Organization Zipcode: 95819
Organization Email: guadalupe.magana@dot.ca.gov
Organization Phone: (916) 227-7302
General Comments for this Test: RTFO
Test Result Compliance: complies
Additional Comments When Verified:
Phase RTFO residue
Test Gap 1 mm
Test Frequency 10.0 rad/s
Strain Amplitude 10.00 %
Stress Amplitude 0.223 kPa
Phase Angle (δ) (for the 10 cycles) 47.8 degree
Complex Modulus (G*) (for the 10 measurements) 2.227 kPa
Test Temperature (Specimen 1) 76.0 C
Dynamic Shear, G*/sin(δ) 3.01 kPa

Test 5 of 17

DIME Test ID: 2022-09-20-1-5
Test Method: AASHTO T315-22: Standard Method of Test for Determining the Rheological Properties of Asphalt Binder Using a Dynamic Shear Rheometer (DSR) (Dynamic Shear)
Verified Date: 09/22/2022
Date Tested: 09/22/2022
Submitted By Organization: CT HQ - Sacramento Asphalt Binder Laboratory
Organization Address: 5900 Folsom Boulevard, Room 225,
Organization City: Sacramento
Organization State: CA
Organization Zipcode: 95819
Organization Email: guadalupe.magana@dot.ca.gov
Organization Phone: (916) 227-7302
General Comments for this Test: PAV
Test Result Compliance: complies
Additional Comments When Verified:
Phase PAV residue
Test Plate Diameter 8 mm
Test Gap 2 mm
Test Frequency 10.0 rad/s
Strain Amplitude 1.00 %
Stress Amplitude 5.744 kPa
Phase Angle (δ) (for the 10 cycles) 55.3 degree
Complex Modulus (G*) (for the 10 measurements) 574.472 kPa
Test Temperature (Specimen 1) 31.0 C
(G*) x sin(δ)= 472 kPa

Test 6 of 17

DIME Test ID: 2022-09-20-1-6
Test Method: AASHTO T350-19: Multiple Stress Creep Recovery (MSCR) Test of Asphalt Binder Using a Dynamic Shear Rheometer (DSR) (Multiple Stress Creep Recovery)
Verified Date: 09/20/2022
Date Tested: 09/20/2022
Submitted By Organization: CT HQ - Sacramento Asphalt Binder Laboratory
Organization Address: 5900 Folsom Boulevard, Room 225,
Organization City: Sacramento
Organization State: CA
Organization Zipcode: 95819
Organization Email: guadalupe.magana@dot.ca.gov
Organization Phone: (916) 227-7302
General Comments for this Test: MCSR
Test Result Compliance: complies
Additional Comments When Verified:
PG test temperature 76.0 C
Average percent recovery at 0.1 kPa 95.6600 %
Average percent recovery at 3.2 kPa 93.0500 %
Nonrecoverable creep compliance 0.0618
Nonrecoverable creep compliance 0.0893
Percent difference between nonrecoverable creep compliance at 0.1 kPa and 3.2 kPa 44.4800 %

Test 7 of 17

DIME Test ID: 2022-09-20-1-7
Test Method: AASHTO T313-22: Standard Method of Test for Determining the Flexural Creep Stiffness of Asphalt Binder Using the Bending Beam Rheometer (BBR)
Verified Date: 09/22/2022
Date Tested: 09/21/2022
Submitted By Organization: CT HQ - Sacramento Asphalt Binder Laboratory
Organization Address: 5900 Folsom Boulevard, Room 225,
Organization City: Sacramento
Organization State: CA
Organization Zipcode: 95819
Organization Email: guadalupe.magana@dot.ca.gov
Organization Phone: (916) 227-7302
General Comments for this Test: BBR #1
Test Result Compliance: complies
Additional Comments When Verified:
Minimum test bath temperature at 240 s -12.1 C
Maximum test bath temperature at 240 s -11.9 C
Time of test load application no data HH:MM:SS
File name of test data no data
Time beam in bath no data
Time test started no data HH:MM:SS
Flags issued by software during test no data
Correlation coefficient (R²) 0
Regression coefficient a no data
Regression coefficient b no data
Regression coefficient c no data
Load at time 0.0 0.0 mN
Deflection at time 0.0 s 0.000 µm
Load at time 0.5 s 0.0 mN
Deflection at time 0.5 s 0.000 µm
Load at 60.0 s 996.0 mN
Beam deflection 60.0 s 0.000 µm
Measured Stiffness Modulus 60.0 s 71.800 mPa
Estimated Stiffness Modulus 60.0 s 71.800 mPa
Difference between stiffness moduli 60.0 s no data
Estimated m-value 60.0 s 0.392

Test 8 of 17

DIME Test ID: 2022-09-20-1-8
Test Method: AASHTO T228-09r13: Standard Method of Test for Specific Gravity of Semi-Solid Asphalt Materials (Specific Gravity)
Verified Date: 09/26/2022
Date Tested: 09/21/2022
Submitted By Organization: CT HQ - Sacramento Asphalt Binder Laboratory
Organization Address: 5900 Folsom Boulevard, Room 225,
Organization City: Sacramento
Organization State: CA
Organization Zipcode: 95819
Organization Email: guadalupe.magana@dot.ca.gov
Organization Phone: (916) 227-7302
General Comments for this Test: Specific Gravity
Test Result Compliance: complies
Additional Comments When Verified:
Specific Gravity 1.007

Test 9 of 17

DIME Test ID: 2022-09-20-1-9
Test Method: AASHTO T315-22: Standard Method of Test for Determining the Rheological Properties of Asphalt Binder Using a Dynamic Shear Rheometer (DSR) (Dynamic Shear)
Verified Date: 09/20/2022
Date Tested: 09/20/2022
Submitted By Organization: CT HQ - Sacramento Asphalt Binder Laboratory
Organization Address: 5900 Folsom Boulevard, Room 225,
Organization City: Sacramento
Organization State: CA
Organization Zipcode: 95819
Organization Email: guadalupe.magana@dot.ca.gov
Organization Phone: (916) 227-7302
General Comments for this Test: OG#2
Test Result Compliance: complies
Additional Comments When Verified:
Phase Original binder
Test Gap 1 mm
Test Frequency 10.0 rad/s
Strain Amplitude 12.00 %
Stress Amplitude 0.156 kPa
Phase Angle (δ) (for the 10 cycles) 46.2 degree
Complex Modulus (G*) (for the 10 measurements) 1.300 kPa
Test Temperature (Specimen 1) 76.0 C
Dynamic Shear, G*/sin(δ) 1.80 kPa

Test 10 of 17

DIME Test ID: 2022-09-20-1-10
Test Method: AASHTO T315-22: Standard Method of Test for Determining the Rheological Properties of Asphalt Binder Using a Dynamic Shear Rheometer (DSR) (Dynamic Shear)
Verified Date: 09/20/2022
Date Tested: 09/20/2022
Submitted By Organization: CT HQ - Sacramento Asphalt Binder Laboratory
Organization Address: 5900 Folsom Boulevard, Room 225,
Organization City: Sacramento
Organization State: CA
Organization Zipcode: 95819
Organization Email: guadalupe.magana@dot.ca.gov
Organization Phone: (916) 227-7302
General Comments for this Test: OG#3
Test Result Compliance: complies
Additional Comments When Verified:
Phase Original binder
Test Gap 1 mm
Test Frequency 10.0 rad/s
Strain Amplitude 12.00 %
Stress Amplitude 0.156 kPa
Phase Angle (δ) (for the 10 cycles) 46.2 degree
Complex Modulus (G*) (for the 10 measurements) 1.300 kPa
Test Temperature (Specimen 1) 76.0 C
Dynamic Shear, G*/sin(δ) 1.80 kPa

Test 11 of 17

DIME Test ID: 2022-09-20-1-11
Test Method: AASHTO T315-22: Standard Method of Test for Determining the Rheological Properties of Asphalt Binder Using a Dynamic Shear Rheometer (DSR) (Dynamic Shear)
Verified Date: 09/20/2022
Date Tested: 09/20/2022
Submitted By Organization: CT HQ - Sacramento Asphalt Binder Laboratory
Organization Address: 5900 Folsom Boulevard, Room 225,
Organization City: Sacramento
Organization State: CA
Organization Zipcode: 95819
Organization Email: guadalupe.magana@dot.ca.gov
Organization Phone: (916) 227-7302
General Comments for this Test: RTFO #2
Test Result Compliance: complies
Additional Comments When Verified:
Phase RTFO residue
Test Gap 1 mm
Test Frequency 10.0 rad/s
Strain Amplitude 10.00 %
Stress Amplitude 0.217 kPa
Phase Angle (δ) (for the 10 cycles) 47.9 degree
Complex Modulus (G*) (for the 10 measurements) 2.167 kPa
Test Temperature (Specimen 1) 76.0 C
Dynamic Shear, G*/sin(δ) 2.92 kPa

Test 12 of 17

DIME Test ID: 2022-09-20-1-12
Test Method: AASHTO T315-22: Standard Method of Test for Determining the Rheological Properties of Asphalt Binder Using a Dynamic Shear Rheometer (DSR) (Dynamic Shear)
Verified Date: 09/20/2022
Date Tested: 09/20/2022
Submitted By Organization: CT HQ - Sacramento Asphalt Binder Laboratory
Organization Address: 5900 Folsom Boulevard, Room 225,
Organization City: Sacramento
Organization State: CA
Organization Zipcode: 95819
Organization Email: guadalupe.magana@dot.ca.gov
Organization Phone: (916) 227-7302
General Comments for this Test: RTFO #3
Test Result Compliance: complies
Additional Comments When Verified:
Phase RTFO residue
Test Gap 1 mm
Test Frequency 10.0 rad/s
Strain Amplitude 10.00 %
Stress Amplitude 0.225 kPa
Phase Angle (δ) (for the 10 cycles) 47.8 degree
Complex Modulus (G*) (for the 10 measurements) 2.255 kPa
Test Temperature (Specimen 1) 76.0 C
Dynamic Shear, G*/sin(δ) 3.04 kPa

Test 13 of 17

DIME Test ID: 2022-09-20-1-13
Test Method: AASHTO T315-22: Standard Method of Test for Determining the Rheological Properties of Asphalt Binder Using a Dynamic Shear Rheometer (DSR) (Dynamic Shear)
Verified Date: 09/22/2022
Date Tested: 09/22/2022
Submitted By Organization: CT HQ - Sacramento Asphalt Binder Laboratory
Organization Address: 5900 Folsom Boulevard, Room 225,
Organization City: Sacramento
Organization State: CA
Organization Zipcode: 95819
Organization Email: guadalupe.magana@dot.ca.gov
Organization Phone: (916) 227-7302
General Comments for this Test: PAV #2
Test Result Compliance: complies
Additional Comments When Verified:
Phase PAV residue
Test Plate Diameter 8 mm
Test Gap 2 mm
Test Frequency 10.0 rad/s
Strain Amplitude 1.00 %
Stress Amplitude 5.738 kPa
Phase Angle (δ) (for the 10 cycles) 55.1 degree
Complex Modulus (G*) (for the 10 measurements) 573.776 kPa
Test Temperature (Specimen 1) 31.0 C
(G*) x sin(δ)= 471 kPa

Test 14 of 17

DIME Test ID: 2022-09-20-1-14
Test Method: AASHTO T315-22: Standard Method of Test for Determining the Rheological Properties of Asphalt Binder Using a Dynamic Shear Rheometer (DSR) (Dynamic Shear)
Verified Date: 09/22/2022
Date Tested: 09/22/2022
Submitted By Organization: CT HQ - Sacramento Asphalt Binder Laboratory
Organization Address: 5900 Folsom Boulevard, Room 225,
Organization City: Sacramento
Organization State: CA
Organization Zipcode: 95819
Organization Email: guadalupe.magana@dot.ca.gov
Organization Phone: (916) 227-7302
General Comments for this Test: PAV #3
Test Result Compliance: complies
Additional Comments When Verified:
Phase PAV residue
Test Plate Diameter 8 mm
Test Gap 2 mm
Test Frequency 10.0 rad/s
Strain Amplitude 1.00 %
Stress Amplitude 6.151 kPa
Phase Angle (δ) (for the 10 cycles) 55.2 degree
Complex Modulus (G*) (for the 10 measurements) 615.117 kPa
Test Temperature (Specimen 1) 31.0 C
(G*) x sin(δ)= 505 kPa

Test 15 of 17

DIME Test ID: 2022-09-20-1-15
Test Method: AASHTO T313-22: Standard Method of Test for Determining the Flexural Creep Stiffness of Asphalt Binder Using the Bending Beam Rheometer (BBR)
Verified Date: 09/22/2022
Date Tested: 09/21/2022
Submitted By Organization: CT HQ - Sacramento Asphalt Binder Laboratory
Organization Address: 5900 Folsom Boulevard, Room 225,
Organization City: Sacramento
Organization State: CA
Organization Zipcode: 95819
Organization Email: guadalupe.magana@dot.ca.gov
Organization Phone: (916) 227-7302
General Comments for this Test: BBR #2
Test Result Compliance: complies
Additional Comments When Verified:
Minimum test bath temperature at 240 s -12.1 C
Maximum test bath temperature at 240 s -11.9 C
Time of test load application no data HH:MM:SS
File name of test data no data
Time beam in bath no data
Time test started no data HH:MM:SS
Flags issued by software during test no data
Correlation coefficient (R²) 0
Regression coefficient a no data
Regression coefficient b no data
Regression coefficient c no data
Load at time 0.0 0.0 mN
Deflection at time 0.0 s 0.000 µm
Load at time 0.5 s 0.0 mN
Deflection at time 0.5 s 0.000 µm
Load at 60.0 s 0.0 mN
Beam deflection 60.0 s 0.000 µm
Measured Stiffness Modulus 60.0 s 73.400 mPa
Estimated Stiffness Modulus 60.0 s 72.800 mPa
Difference between stiffness moduli 60.0 s no data
Estimated m-value 60.0 s 0.412

Test 16 of 17

DIME Test ID: 2022-09-20-1-16
Test Method: AASHTO T301-22: Standard Method of Test for Elastic Recovery Test of Asphalt Materials by Means of a Ductilometer
Verified Date: 09/22/2022
Date Tested: 09/21/2022
Submitted By Organization: CT HQ - Sacramento Asphalt Binder Laboratory
Organization Address: 5900 Folsom Boulevard, Room 225,
Organization City: Sacramento
Organization State: CA
Organization Zipcode: 95819
Organization Email: guadalupe.magana@dot.ca.gov
Organization Phone: (916) 227-7302
General Comments for this Test:
Test Result Compliance: complies
Additional Comments When Verified:
% Elongation Recovery 96 %

Test 17 of 17

DIME Test ID: 2022-09-20-1-17
Test Method: AASHTO T301-22: Standard Method of Test for Elastic Recovery Test of Asphalt Materials by Means of a Ductilometer
Verified Date: 09/22/2022
Date Tested: 09/21/2022
Submitted By Organization: CT HQ - Sacramento Asphalt Binder Laboratory
Organization Address: 5900 Folsom Boulevard, Room 225,
Organization City: Sacramento
Organization State: CA
Organization Zipcode: 95819
Organization Email: guadalupe.magana@dot.ca.gov
Organization Phone: (916) 227-7302
General Comments for this Test:
Test Result Compliance: complies
Additional Comments When Verified:
% Elongation Recovery 95 %