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Sample Record for 2021-04-05-23

Note: Fields with no data or with a value of "Unknown" will not be displayed on the print out.

Project Information

Project ID: 44444 DEA: ASCP EFIS: ASCP QA Service Level:
DIST-CO-RTE-PM: 59---
Work Description: Special project for submitting Sample information for Asphalt Supplier Certification Program.
Location Description:
Contractor Name: Unknown
Contractor Address: Unknown
Resident Engineer: Unknown Structure Rep.: Unknown

Sample Information

DIME Sample ID: 2021-04-05-23
TL Number from the TL Form:
Sample Submitted By Organization: Valero-NuStar PAT - Pittsburg
Sample Organization Contact: (707) 745-7089
Type of Sample: Quality Control
Type of Material: Asphalt Binder
Sample Taken Date: 04/05/2021
Date that the sample was received by the laboratory/organization performing the testing: 04/07/2021
The quantity of what the sample constitutes: 1 of 2 split sample
A brief description of the sample: Asphalt Binder PG 76-22M
From where was the sample collected: Manufacturer
Laboratory sample identification: 7622M-040521
Structure unique identifier:
Structure name:
The fabricator/manufacturer/facility name: Valero Pittsburg

Material Information

Performance Grade: PG 76-22 M
Modified: Yes
Lot number:
Sublot number:
Tank number: 5001
Time of sample:
HMA Supplier:
Certified Asphalt Supplier: Valero-NuStar PAT - Pittsburg CA
Multigrade: No
Multigrade Type:
Asphalt Binder Mix Number:
Test results on following page(s): 9

Test Results

Test 1 of 9

DIME Test ID: 2021-04-05-23-1
Test Method: AASHTO R28-16: Accelerated Aging of Asphalt Binder Using a Pressurized Aging Vessel (PAV)
Verified Date: 04/30/2021
Date Tested: 04/08/2021
Submitted By Organization: Valero-NuStar PAT - Pittsburg
Organization Address: 1100 Willow Pass Road,
Organization City: Pittsburg
Organization State: CA
Organization Zipcode: 94565
Organization Email: patrick.sendegeya@valero.com
Organization Phone: (707) 745-7214
General Comments for this Test:
Test Result Compliance:
Additional Comments When Verified:
Sample identification 7622M040521
Aging Test Temperature, nearest 0.5 C 110 C
Minimum aging temperature recorded 110 C
Maximum aging temperature recorded 110 C
Total time during aging that temperature was outside the specified range 1 minutes
Total aging time (hour) 20 hours
Total aging time (minute) no data0 minutes
The heating temperature 110 C

Test 2 of 9

DIME Test ID: 2021-04-05-23-2
Test Method: AASHTO T240-17: Standard Method of Test for Effect of Heat and Air on a Moving Film of Asphalt Binder (Rolling Thin-Film Oven Test)
Verified Date: 04/30/2021
Date Tested: 04/07/2021
Submitted By Organization: Valero-NuStar PAT - Pittsburg
Organization Address: 1100 Willow Pass Road,
Organization City: Pittsburg
Organization State: CA
Organization Zipcode: 94565
Organization Email: patrick.sendegeya@valero.com
Organization Phone: (707) 745-7214
General Comments for this Test:
Test Result Compliance:
Additional Comments When Verified:
Is mass change based on one or two containers? Two
Average mass change -0.419 percent

Test 3 of 9

DIME Test ID: 2021-04-05-23-3
Test Method: AASHTO T301-13: Standard Method of Test for Elastic Recovery Test of Asphalt Materials by Means of a Ductilometer
Verified Date: 04/30/2021
Date Tested: 04/07/2021
Submitted By Organization: Valero-NuStar PAT - Pittsburg
Organization Address: 1100 Willow Pass Road,
Organization City: Pittsburg
Organization State: CA
Organization Zipcode: 94565
Organization Email: patrick.sendegeya@valero.com
Organization Phone: (707) 745-7214
General Comments for this Test:
Test Result Compliance:
Additional Comments When Verified:
% Elongation Recovery 75 %

Test 4 of 9

DIME Test ID: 2021-04-05-23-4
Test Method: AASHTO T313-19: Standard Method of Test for Determining the Flexural Creep Stiffness of Asphalt Binder Using the Bending Beam Rheometer (BBR)
Verified Date: 04/30/2021
Date Tested: 04/09/2021
Submitted By Organization: Valero-NuStar PAT - Pittsburg
Organization Address: 1100 Willow Pass Road,
Organization City: Pittsburg
Organization State: CA
Organization Zipcode: 94565
Organization Email: patrick.sendegeya@valero.com
Organization Phone: (707) 745-7214
General Comments for this Test:
Test Result Compliance:
Additional Comments When Verified:
Time test started no data HH:MM:SS
Flags issued by software during test no data
Correlation coefficient (R²) no data0
Regression coefficient a no data
Regression coefficient b no data
Regression coefficient c no data
Load at time 0.0 no data0 mN
Deflection at time 0.0 s no data0 µm
Load at time 0.5 s no data0 mN
Deflection at time 0.5 s no data0 µm
Load at 60.0 s no data0 mN
Beam deflection 60.0 s no data0 µm
Measured Stiffness Modulus 60.0 s 116.5 mPa
Estimated Stiffness Modulus 60.0 s 116.5 mPa
Difference between stiffness moduli 60.0 s no data
Estimated m-value 60.0 s 0.348

Test 5 of 9

DIME Test ID: 2021-04-05-23-5
Test Method: AASHTO T315-16: Standard Method of Test for Determining the Rheological Properties of Asphalt Binder Using a Dynamic Shear Rheometer (DSR) (Dynamic Shear)
Verified Date: 04/30/2021
Date Tested: 04/07/2021
Submitted By Organization: Valero-NuStar PAT - Pittsburg
Organization Address: 1100 Willow Pass Road,
Organization City: Pittsburg
Organization State: CA
Organization Zipcode: 94565
Organization Email: patrick.sendegeya@valero.com
Organization Phone: (707) 745-7214
General Comments for this Test:
Test Result Compliance:
Additional Comments When Verified:
Phase Original binder
Test Plate Diameter 25 mm
Phase Angle (δ) (for the 10 cycles) 73.2 degree
Dynamic Shear, G*/sin(δ) 1.29 kPa

Test 6 of 9

DIME Test ID: 2021-04-05-23-6
Test Method: AASHTO T315-16: Standard Method of Test for Determining the Rheological Properties of Asphalt Binder Using a Dynamic Shear Rheometer (DSR) (Dynamic Shear)
Verified Date: 04/30/2021
Date Tested: 04/07/2021
Submitted By Organization: Valero-NuStar PAT - Pittsburg
Organization Address: 1100 Willow Pass Road,
Organization City: Pittsburg
Organization State: CA
Organization Zipcode: 94565
Organization Email: patrick.sendegeya@valero.com
Organization Phone: (707) 745-7214
General Comments for this Test: DSR RTFO also run at 82C to make determine Calculated Delta at 68.5.
Test Result Compliance:
Additional Comments When Verified:
Phase RTFO residue
Test Plate Diameter 25 mm
Phase Angle (δ) (for the 10 cycles) 67.9 degree
Dynamic Shear, G*/sin(δ) 2.47 kPa

Test 7 of 9

DIME Test ID: 2021-04-05-23-7
Test Method: AASHTO T315-16: Standard Method of Test for Determining the Rheological Properties of Asphalt Binder Using a Dynamic Shear Rheometer (DSR) (Dynamic Shear)
Verified Date: 04/30/2021
Date Tested: 04/09/2021
Submitted By Organization: Valero-NuStar PAT - Pittsburg
Organization Address: 1100 Willow Pass Road,
Organization City: Pittsburg
Organization State: CA
Organization Zipcode: 94565
Organization Email: patrick.sendegeya@valero.com
Organization Phone: (707) 745-7214
General Comments for this Test:
Test Result Compliance:
Additional Comments When Verified:
Phase PAV residue
Test Plate Diameter 8 mm
Phase Angle (δ) (for the 10 cycles) 46.0 degree
(G*) x sin(δ)= 1380 kPa

Test 8 of 9

DIME Test ID: 2021-04-05-23-8
Test Method: AASHTO T316-17: Standard Method of Test for Viscosity Determination of Asphalt Binder Using Rotational Viscometer
Verified Date: 04/30/2021
Date Tested: 04/07/2021
Submitted By Organization: Valero-NuStar PAT - Pittsburg
Organization Address: 1100 Willow Pass Road,
Organization City: Pittsburg
Organization State: CA
Organization Zipcode: 94565
Organization Email: patrick.sendegeya@valero.com
Organization Phone: (707) 745-7214
General Comments for this Test:
Test Result Compliance:
Additional Comments When Verified:
Is viscosity reading in cP/Pa-s? Pa-s
Time of test 12:00 HH:MM
Test Temperature 135 C
Speed 20 rpm
Spindle size S21 in
Torque 50 %
Viscosity reading #1 (A) 1.256 Pa-s
Viscosity reading #2 (B) 1.26 Pa-s
Viscosity reading #3 (C) 1.262 Pa-s
Average viscosity 1.259 Pa-s

Test 9 of 9

DIME Test ID: 2021-04-05-23-9
Test Method: AASHTO T48-18: Standard Method of Test for Flash Point of Asphalt Binder by Cleveland Open Cup
Verified Date: 04/30/2021
Date Tested: 04/07/2021
Submitted By Organization: Valero-NuStar PAT - Pittsburg
Organization Address: 1100 Willow Pass Road,
Organization City: Pittsburg
Organization State: CA
Organization Zipcode: 94565
Organization Email: patrick.sendegeya@valero.com
Organization Phone: (707) 745-7214
General Comments for this Test:
Test Result Compliance:
Additional Comments When Verified:
Units of measurement for Observed Flash Point (C or F) and Ambient barometric pressure (kP or mmHg) Celsius and mmHg
Observed Flash Point 306 C
Ambient Barometric Pressure 752 mmHg
Cleveland Open-Cup Flash Point in Celsius 306 C